Inductively Coupled Plasma

Presentation

The “Plasma Torch Spectrometry” instrumental cluster allows the measurement of concentrations of metallic and organometallic species in solid* and liquid matrices such as water, aerosols, sediment, soil, and plants. The tools available in the division can also be used in many other fields, such as materials, food industry, and health.

*Solid matrices require a prior dissolution step.

For any analysis request, please send an email to the following address: analyse-de-traces_at_univ-lille.fr

Location 
(D9) Chevreul Institute Building – Cité Scientifique
59655 Villeneuve d’Ascq, France

For new requests, please complete the project form before contacting the division.

ICP usage procedure (PDF)

 

 

Staff:

  • David Dumoulin (Scientific Head of the cluster)
  • Véronique Alaimo (Technical Head of the cluster)
  • Gabriel Billon (Advisory Support)

ICP-OES Agilent 5110

This atomic emission spectrometer coupled with a plasma torch allows the simultaneous analysis of major and trace elements in solution, with detection limits on the order of a few μg L⁻¹.

 

Sample Changer SPS4
Sample Introduction Nebulizers: OneNeb, Seaspray, Concentric

Double-pass Cyclonic Chamber

Inert Kit for HF Matrices
Plasma Vertical torch

Power: 700 to 1500 W
Detection Dual view (axial and radial)

CCD (167-765 nm)

ICP-MS Agilent 7850

The quadrupole mass spectrometer coupled with a plasma torch (ICP-MS) Agilent 7850 achieves detection limits often below µg L⁻¹ and allows the analysis of trace and ultra-trace elements across a wide range of applications.

 

Sample Changer SPS4
Sample Introduction Concentric micro-nebulizer

Scott Chamber: Peltier-cooled

Gas Dilution (UHMI)

Plasma Shield Torch System

Power: 500 to 1600 W
Ion Optics Off-axis lenses
Interference Management Octopole collision/reaction cell

Available gases: He, H₂

Kinetic energy discrimination

Detection Orthogonal electron multiplier with discrete dynodes

Linear Dynamic Range: 10 orders of magnitude

ICP-MS Agilent 7900

The Agilent 7900 is a next-generation quadrupole ICP-MS dedicated to ultra-trace analyses and speciation studies when coupled with chromatographic tools (HPLC and GC).

 

Sample Changer SPS4
Sample introduction

Concentric micro-nebulizer

Desolvator (APEX HF)

Scott Chamber : Peltier-cooled

Gas Dilution (UHMI)

Coupling: HPLC (Agilent 1260 Bioinert) and GC (Agilent 7890B)

Plasma Shield Torch System

Power 500 to 1600 W
Ion Optics Off-axis lenses
Interference Management Octopole collision/reaction cell

Available gases: He, H₂, O₂

Kinetic energy discrimination

Detection Orthogonal electron multiplier with discrete dynodes

Linear Dynamic Range : 11 orders of magnitude